Analysis Methods for Development of Standard Reference Material (SRM) Zircon Minerals Synthesis

https://doi.org/10.22146/ijc.25194

Samin Samin(1*), Susanna Tuning Sunanti(2)

(1) Department of Process Technology, Center for Accelerator Science and Technology - BATAN
(2) Department of Process Technology, Center for Accelerator Science and Technology - BATAN
(*) Corresponding Author

Abstract


The synthesis method of in-house zircon minerals certified reference material (CRM) from Kalimantan (Tumbang Titi), and Bangka has been studied with statistical method of ISO 13528-2008 and ISO 35-2006. Zircon Minerals weighing of 10 kg, and it was dried at 90 °C for 2 × 6 h in a closed room, then crushed with a Ball-Mill up to passes 200 mesh, and homogenized in a homogenizer for 3 × 6 h. The water content in zircon minerals powder is tested by gravimetric method, whereas the homogeneity and stability assessed by statistical methods. Zircon mineral powders are distributed to seven accredited testing laboratory for testing the composition and content of the oxides with the validated analytical methods. Standardization and characterization of candidate zircon mineral certified reference materials are done by using XRD (X-Ray Diffraction) and used standard materials of JCRM R 502 from Japan. The test results of oxide concentrations from various laboratories processed with statistical methods. From the data by test laboratories obtained 40 bottles of the prototype in-house certified reference materials zircon mineral powders from Kalimantan and Bangka with a capacity of 100 g. Based on standardization and characterization test data obtained a major chemical compound on zircon minerals Kalimantan and Bangka similar to the standard that is ZrSiO4. This in-house CRM is traced to certified reference materials from Japan (JCRM-502).

Keywords


in-house CRM; zirconium minerals; reference materials



References

[1] Purwastien, P., Judprasong, K., and Pinprapai, N., 2009, Development of rice reference material and its use for evaluation of analytical performance of food analysis laboratories, J. Food Compos. Anal., 22, 453–462.

[2] Guimarães, E.F., do Rego, E.C.P., Cunha, H.C.M., Rodrigues, J.M., and Figueroa-Villar, J.D., 2014, Certified reference material for traceability in environmental analysis: PAHs in toluene, J. Braz. Chem. Soc., 25 (2), 351–360.

[3] Quan, C., Yao, H., and Hou, C., 2013, Certification and uncertainty evaluation of flavonoids certified reference materials, J. Agric. Sci., 4 (9B), 89–96.

[4] McCarron, P., Reeves, K.L., Giddings, S.D., Beach, D.G., and Quilliam, M.A., 2016, Development of certified reference materials for diarrhetic shellfish poisoning toxins, part 2: Shellfish matrix materials, J. AOAC Int., 99 (5), 1163–1172.

[5] Nogueira, R., do Rego, E.C.P., Sousa, M.V.B., Wollinger, W., da Silva, T.E., Moreira, G.F., Barin, J.M., Laporta, L.V., Mesko, M.F., Bittencourt, C.F., Rodrigues, J.M., and da Cunha, V.S., 2011, Development studies of captopril certified reference material, Braz. J. Pharm. Sci., 47 (2), 339–350.

[6] Dai, X., Fang, X., Shao, M., Li, M., Huang, Z., Li, H., Jiang, Y., Song, D., and He, Y., 2011, Corrigendum to “certified reference materials (GBW09170 and 09171) of creatinine in human serum”, J. Chromatogr. B, 879 (20), 1845.

[7] Magharbeh, M., Fayyad, M., and Bartarseh, M., 2012, Preparation of natural standard reference material (SRM) for El-lajjun oil shale/Jordan, Jordan J. Earth .Environ. Sci., 4 (2), 15–22.

[8] Rimmer, C.A., Putzbach, K., Sharpless, K.E., Sander, L.C., and Yen, J.H., 2012, Preparation and certification of standard reference material 3278 tocopherols in edible oils, J. Agric. Food Chem., 60 (27), 6794–6798

[9] Portugal, T.R., Parcon, M.R.V., and Udarbe, M.A., 2013, Proficiency test on total dietary fiber in wheat flour, Int. J. Chem. Eng. Appl., 4 (2), 82–87.

[10] Bebić, J.M., Gažević, L.S., and Bläul, C., 2016, Prolab software for data evaluation of interlaboratory studies, Int. J. Adv. Qual., 44 (3), 23–28.

[11] Ahadnejad, V., Valizadeh, M.V, Esmaeily D., and Bokani, S.J., 2008, Setting in-house XRF reference material for minerals; A case study: Botite minerals or malayer granitoid rocks (Western Iran), J. Appl. Sci., 8 (23), 4369–4375.

[12] Jedziniak, P., Szprengier-Juszkiewicz, T., and Olejnik, M., 2009, In-house reference materials: 5-hydroxyflunixin and meloxicam in cow milk-preparation and evaluation, Anal. Chim. Acta, 637 91-2), 346–350.

[13] Ulrich, J.C., Sarkis, J.E.S., and Hortellani, M.A., 2015, Homogeneity study of candidate reference material in fish matrix, J. Phys. Conf. Ser., 575, 012040.

[14] Korpysa-Dzirba, W., Rola, J.G., and Osek, J., 2012, Homogeneity and stability of samples used for proficiency testing in enumeration of coagulase positive staphylococci, Bull Vet. Inst. Pulawy, 56 (4), 559–562.

[15] Taftazani, A., Prihatin, S., Sunanti, S.T., Suprianto, C., and Suratman, S., 2012, Preparation of certified reference materials (CRMs) zircon sand, 13th International Symposium on Biological and Environmental Reference Materials (BERM 13), Vienna, Austria.

[16] ISO Guide 35, 1989, Certification of reference Materials - General and statistic principles.

[17] British Chemical Standard-Reference Material, 1991, Zircon, Analysis Report, BCS-RM No. 204a.

[18] British Chemical Standard-Reference Material, 2015, Zircon, Certificate of Analysis, BCS-RM No. 388.



DOI: https://doi.org/10.22146/ijc.25194

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