ISOLATION AND IDENTIFICATION FLAVONOID COMPOUND FROM THE STEM BARK OF Saccopetalum horsfieldii BENN

https://doi.org/10.22146/ijc.21738

Mahmiah Mahmiah(1*)

(1) Laboratory of Chemistry, Hang Tuah University, Jl. Arif Rahman Hakim 150 Surabaya
(*) Corresponding Author

Abstract


Isolation and identification flavonoid compound from the stem bark of Indonesian plant Saccopetalum horsfieldii Benn. Annonaceae family have been done. Extraction was carried out by maseration method using methanol at room temperature, the product was then extracted by n-hexane and etil acetate. Etil acetate extract separation carried out by liquid vacuum column chromatography and flash column chromatography. The product purificated by recristalization using acetone p.a. into yellow solid that having melting point of 224-226 °C. The structure of flavonoid compound was determinated by spectroscopy method : UV-vis, IR, 1H-NMR and 12C-NMR. The flavonoid compound known as quercetin-3,7-dimetil eter or 3,7-dimetoksi quercetin.


Keywords


Saccopetalum horsfieldii Benn; flavonoid; chromatography; quercetin

Full Text:

Full Text Pdf


References

[1] Harborne, J,B, 1987, Metode Fitokimia, Penuntun Cara Modern Menganalisis Tumbuhan (diterjemahkan oleh K. Panduwinata dan Soediro, I.), terbitan ke-2, Penerbit ITB, Bandung.

[2] Heyne, K, 1987, Tumbuhan Berguna Indonesia (diterjemahkan oleh Badan Litbang Kehutanan), Jilid III, Edisi ke-2, Penerbit Yayasan Wanajaya, Jakarta.

[3] Hakim, E.H., Achmad, S.A., Makmur, L., Mujahidin, D., and Syah, Y.M., 2001, Bull. Indo. Soc. Nat. Prod. Chem., 1, 1-10.

[4] Hegnauer, R., 1969, Chemotaxonomie der Planzen III, 116-123.

[5] Utomo, P., 2002, Isolasi dan Identifikasi Senyawa Lignan dari kulit Batang Tanaman Saccopetalum horsfieldii BENN, Skripsi, Jurusan Kimia, FMIPA, UNAIR, Surabaya.

[6] Fatatik, R., 2002, Isolasi dan Identifikasi Senyawa Fenolik dari kulit Batang Tanaman Saccopetalum horsfieldii BENN, Skripsi, Jurusan Kimia, FMIPA, UNAIR, Surabaya.

[7] Wibowo, A., 2002, Isolasi dan Identifikasi Senyawa Flavonoid dari kulit Batang Saccopetalum horsfieldii BENN, Skripsi, Jurusan Kimia, FMIPA, UNAIR, Surabaya.

[8] Markham, K.R., 1998, Cara Mengidentifikasi Flavonoid, Penerbit ITB, Bandung.

[9] Masruroh, and Siti, M.R., 2003, Isolasi dan Identifikasi Senyawa Flavonoid Fraksi Diklorometana dari Kulit Batang Saccopetalum horsfieldii Benn., Skripsi, Jurusan Kimia, FMIPA, Universitas Airlangga, Surabaya.

[10]Silverstein, R.M, Bassler, G.c, and Morril, T.C, 1991, Spectrometric Identification of Organic Compound, Fifth Edition, John Wiley, Inc, Toronto.



DOI: https://doi.org/10.22146/ijc.21738

Article Metrics

Abstract views : 2277 | views : 8486


Copyright (c) 2010 Indonesian Journal of Chemistry

Creative Commons License
This work is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.

 


Indonesian Journal of Chemistry (ISSN 1411-9420 /e-ISSN 2460-1578) - Chemistry Department, Universitas Gadjah Mada, Indonesia.

Web
Analytics View The Statistics of Indones. J. Chem.